METHOD OF PRODUCING VALIDOL Russian patent published in 2017 - IPC C07C69/03 C07C67/08 

Abstract RU 2626978 C1

FIELD: chemistry.

SUBSTANCE: esterification of isovaleric acid with menthol is performed in the presence of sulfuric acid during heating followed by washing and vacuum distillating, where the washing is carried out in succession with purified water, 3% sodium hydroxide solution and 25% sodium chloride solution, the mentyl isovalerate-raw in the presence of soda calcined to produce three fractions. Menthol is added to the second fraction and the resulting solution is heated to a temperature of 30-50°C, maintained for 1-1.5 hours with stirring and then cooled.

EFFECT: method allows to produce cleaner product with fewer by-products.

2 cl, 1 ex

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RU 2 626 978 C1

Authors

Solodukhina Lyudmila Aleksandrovna

Abrosimova Lyudmila Aleksandrovna

Dates

2017-08-02Published

2016-03-10Filed