FIELD: chemistry.
SUBSTANCE: invention relates to a method of producing benzanilide. Method is carried out by reacting benzoic acid with aniline in medium of absolute acetonitrile in presence of complex obtained in situ from phosphorus trichloride with 4-dimethylaminopyridine, taken in molar ratio: 1:1. Reaction is carried out in molar ratio acid: amine: complex equal to 2.5:5–7.5:1.
EFFECT: technical result is simple method of producing benzanilide and increasing its output.
1 cl, 2 ex
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD OF PRODUCING AROMATIC AMIDES OF 1-ADAMANTANE CARBOXYLIC ACID | 2019 |
|
RU2698193C1 |
| METHOD OF PRODUCING CARBOXYLIC ACID AMIDES | 2014 |
|
RU2565059C1 |
| METHOD OF REAMIDATING AMIDES OF CARBOXYLIC ACIDS | 2014 |
|
RU2558366C1 |
| METHOD OF PRODUCING CYCLOALKYLAMINES | 2010 |
|
RU2425828C1 |
| WAY OF AMINE ACIDYLATION | 2010 |
|
RU2442770C1 |
| METHOD FOR PRODUCING CIS-MIRTANOL ACID | 2021 |
|
RU2756658C1 |
| LOW MOLECULAR WEIGHT LIGANDS OF ASIALOGLYCOPROTEIN RECEPTOR BASED ON QUINOLINE-4-CARBOXYLIC ACID | 2020 |
|
RU2769859C1 |
| METHOD OF THE PRODUCTION OF PARA-ACETYLAMINOPHENOL | 2022 |
|
RU2800098C1 |
| METHOD FOR PRODUCING 4-N,N-DIMETHYLAMINOPYRIDINE | 2020 |
|
RU2733717C1 |
| METHOD OF PRODUCING ETHYL ETHER OF 3-OXO-3-(2,6-DICHLOROPYRIDIN-3-YL) PROPANOIC ACID | 2010 |
|
RU2435758C1 |
