FIELD: technological processes.
SUBSTANCE: invention relates to a method of applying nanostructured and wear-resistant coatings from high-entropy alloys with thermoelastic phase transformations by magnetron-plasma sputtering. Part surface is etched with low-temperature argon plasma at pressure 150-250 Pa for 5-10 minutes. Then, target surface is cleaned consisting of high-entropy FeNiCoAlX alloy, where X is impurity alloying or dopant component in form of Ti, Ta, Nb, Cr or W. Target contains components at following ratio, wt.%: Fe - 41-43, Ni - 28-30, Co - 15-17, Al - 10-11.5, X - 2-2.5. Upper layer of the target is sprayed on flap for 1-2 minutes at a plasma current of 150-200 mA with voltage of 370-420 V. Flap is then removed. Ion-plasma spraying of coating on part with thickness of 500-700 nm is performed at pressure of 1.5-2.5 Pa, plasma current is 110-130 mA and voltage is 350-450. Further, phase-forming thermal annealing is carried out in an inert atmosphere of argon at temperature of 573-773 K for 40-80 minutes.
EFFECT: technical result is higher resistance to abrasive, hydroabrasive and cavitation wear, and resistance to fatigue cracking coating at operating temperatures below 273 K.
1 cl, 1 tbl, 15 ex, 3 dwg
| Title | Year | Author | Number | 
|---|---|---|---|
| METHOD OF PRODUCING A WEAR-RESISTANT COATING OF A CUTTING TOOL | 2019 | 
 | RU2699418C1 | 
| METHOD OF PRODUCING A WEAR-RESISTANT COATING OF A CUTTING TOOL | 2019 | 
 | RU2718642C1 | 
| METHOD FOR HYBRID OBTAINING OF WEAR-RESISTANT COATING ON CUTTING TOOL | 2011 | 
 | RU2485210C2 | 
| METHOD OF PRODUCING WEAR-RESISTANT COATING ON CUTTING TOOL | 2023 | 
 | RU2827193C1 | 
| METHOD FOR VACUUM-ARC DEPOSITION OF NANOSTRUCTURED COATINGS ON DENTAL STRUCTURES | 2022 | 
 | RU2791571C1 | 
| METHOD FOR PRODUCING ANTI-CORROSIVE COATING ON ARTICLES FROM MONOLITHIC TITANIUM NICKELIDE | 2020 | 
 | RU2751704C1 | 
| METHOD OF ION-PLASMA TREATMENT OF STEEL AND HARD ALLOY PARTS | 2008 | 
 | RU2370570C1 | 
| METHOD OF COMBINED PLASMA SURFACE TREATMENT OF ITEMS FROM TITANIUM ALLOYS | 2017 | 
 | RU2671026C1 | 
| PROCEDURE FOR PRODUCTION OF NANO STRUCTURED GRADIENT OXIDE COATING OF CATALYTIC MATERIAL BY METHOD OF MAGNETRON SPUTTERING | 2009 | 
 | RU2428516C2 | 
| METHOD OF PRODUCING PLATINUM-BASED CATALYST AND PLATINUM-BASED CATALYST | 2014 | 
 | RU2562462C1 | 
Authors
Dates
2021-02-10—Published
2020-07-14—Filed