METHOD FOR PRODUCING FERRITE FILMS Russian patent published in 2023 - IPC C23C14/28 C23C14/46 C23C14/08 C23C14/02 C23C14/54 C23C14/58 C01F11/02 C01G49/02 H01F1/10 H01F10/20 H01F10/28 

Abstract RU 2790266 C1

FIELD: synthesis technology.

SUBSTANCE: invention relates to a technology for the synthesis of anisotropic (with an easy magnetization axis directed perpendicular to the film plane) BaFe12O19 films by vapor phase deposition. Such a material can be used in the development of planar nonreciprocal microwave devices with a self-bias effect, in spintronic devices as a magnetic dielectric. The method for obtaining ferrite films includes the production of a target, treatment of a single-crystal substrate with argon ions, sputtering of the target onto a heated substrate, supply of a controlled flow of oxygen ions to the substrate area, further crystallization annealing of the film, while a target of the same composition, a single-crystal substrate, is used to obtain a film of barium hexaferrite BaFe12O19 Al2O3 crystallographic orientation (001), the substrate is heated to a temperature of 300-350°C during the deposition process, after deposition of a 70-90 nm film on the substrate, the deposition process is interrupted, after which the film is held for 5 minutes at the substrate temperature, then the deposition is repeated many times layers of 70-90 nm and exposure at a temperature of 300-350°C for 5 min until the required film thickness, and crystallization annealing is carried out in air at a temperature of 800-900°C for 1-3 hours.

EFFECT: obtaining high-quality thick (up to ~1 μm and more) anisotropic films of hexagonal ferrites BaFe12O19 with the direction of the magnetic moment perpendicular to the plane of the film.

1 cl, 3 dwg, 1 ex

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RU 2 790 266 C1

Authors

Mironovich Andrej Yurevich

Isaev Igor Magomedovich

Kostishin Vladimir Grigorevich

Timofeev Andrej Vladimirovich

Shakirzyanov Rafael Iosifovich

Korovushkin Vladimir Vasilevich

Shcherbakov Sergej Vladilenovich

Nalogin Aleksej Grigorevich

Alekseev Albert Aleksandrovich

Dates

2023-02-15Published

2022-04-22Filed