METHOD OF PRODUCING NANOPOWDERS OF POROUS SILICON Russian patent published in 2020 - IPC C01B33/21 C30B29/06 C25B1/00 C25F3/12 B82B3/00 B82Y5/00 B82Y40/00 A61K9/14 

Abstract RU 2722098 C1

FIELD: medicine; technological processes.

SUBSTANCE: invention relates to production of nanopowders of silicon and can be used in dentistry and biomedicine for production of photoluminescent labels. Method of producing nanopowders of porous silicon involves etching with acidified concentrated sulphuric acid to pH 4 with an aqueous solution of ammonium fluoride NH4F of monocrystalline silicon in a cell of electrochemical anodic etching with a stainless steel counter electrode, washing the obtained porous material in distilled water, mechanically separating from the crystalline substrate, grinding, drying the obtained powder in natural conditions, wherein aqueous solution of ammonium fluoride NH4F is used with concentration equal to 40 %.

EFFECT: technical result consists in obtaining nanopowder of porous silicon, which exhibits high-intensity photoluminescence when excited by a source with wavelength of 337 nm and higher using a less toxic aqueous solution of ammonium fluoride while maintaining high efficiency of the process.

1 cl, 5 dwg

Similar patents RU2722098C1

Title Year Author Number
METHOD OF PRODUCING POROUS SILICON PRODUCTION 2017
  • Lenshin Aleksandr Sergeevich
  • Kashkarov Vladimir Mikhajlovich
  • Seredin Pavel Vladimirovich
RU2652259C1
METHOD OF OBTAINING POWDER OF POROUS SILICON 2014
  • Len'Shin Aleksandr Sergeevich
  • Kashkarov Vladimir Mikhajlovich
  • Seredin Pavel Vladimirovich
RU2572128C1
METHOD OF PRODUCTION OF POWDERS OF POROUS SILICON 2014
  • Len'Shin Aleksandr Sergeevich
  • Kashkarov Vladimir Mikhajlovich
  • Seredin Pavel Vladimirovich
RU2572134C1
PRODUCTION OF POROUS SILICON WITH STABLE PHOTO LUMINESCENCE 2014
  • Mel'Nik Nikolaj Nikolaevich
  • Tregulov Vadim Viktorovich
RU2568954C1
METHOD FOR PREPARING WATER SUSPENSION OF BIOCOMPATIBLE POROUS SILICON PARTICLE 2012
  • Timoshenko Viktor Jur'Evich
  • Osminkina Ljubov' Andreevna
  • Zajtsev Vladimir Borisovich
  • Bazylenko Tat'Jana Jur'Evna
RU2504403C1
METHOD OF PRODUCING POROUS CERAMIC BIOCOMPATIBLE NANOCARRIERS 2014
  • Sul'Din Aleksandr Vladimirovich
  • Doronin Aleksandr Nikolaevich
RU2553913C1
ELECTROLYTE FOR PRODUCING POROUS SILICON 2000
  • Korsakov V.S.
  • Plavich L.A.
  • Borisov A.G.
  • Vasenkov A.A.
  • Mazurenko S.N.
  • Samsonov N.S.
  • Trutnev N.F.
RU2194805C2
METHOD FOR PRODUCING POROUS PHOTOLUMINESCENT SILICON 2006
  • Shelonin Evgenij Aleksandrovich
  • Khort Andrej Mikhajlovich
  • Nikulin Dmitrij Sergeevich
  • Jakovenko Anatolij Georgievich
RU2316077C1
METHOD OF PRODUCING NANOCRYSTALLINE SILICON HAVING STABLE, BRIGHT PHOTOLUMINESCENCE 2009
  • Ishchenko Anatolij Aleksandrovich
  • Dorofeev Sergej Gennadievich
  • Kononov Nikolaj Nikolaevich
  • Ol'Khov Anatolij Aleksandrovich
RU2411613C1
METHOD OF FORMING LAYER OF POROUS SILICON ON CRYSTALLINE SUBSTRATE 2017
  • Mantuzov Anton Viktorovich
  • Potapova Galina Filippovna
  • Vorontsov Pavel Sergeevich
  • Ryndya Sergej Mikhajlovich
  • Putilov Aleksandr Valentinovich
RU2703909C2

RU 2 722 098 C1

Authors

Lenshin Aleksandr Sergeevich

Kashkarov Vladimir Mikhajlovich

Seredin Pavel Vladimirovich

Dates

2020-05-26Published

2019-08-02Filed