METHOD OF OBTAINING GLASS WITH ANTIREFLECTION MESOPOROUS COATING BASED ON SiO NANOPARTICLES Russian patent published in 2014 - IPC C03C17/25 

Abstract RU 2503629 C1

FIELD: chemistry.

SUBSTANCE: invention relates to thin-film clarifying coatings on glass and can be applied in glass industry and electronics. Method of obtaining glass with antireflection mesoporous coating based on SiO2 nanoparticles, includes preliminary preparation of glass substrate, preparation of silicasol with average diameter of particles 100 nm and low polydispersion, application of SiO2 nanoparticles on glass substrate, thermal procession of coated glass. To improve coating adhesion to glass by functionalisation and creation of electrostatic interaction between substrate and coating glass is kept in 1% solution of 3-aminopropyltriethyloxysilane in ethanol (ω=96%) for 5-15 hours, dried in argon atmosphere, with layers of SiO2 nanoparticles being applied from silicasol, synthesised from tetraethoxysilane in ethyl alcohol in presence of alkaline catalyst with molar component ratio TEOS/C2H5OH/NH4OH/H2O=0.25/8/0.1/1.3.

EFFECT: obtaining antireflection coatings based on SiO2 nanoparticles which have high adhesion to glass surface.

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RU 2 503 629 C1

Authors

Es'Kin Stanislav Viktorovich

Kosobudskij Igor' Donatovich

Zhimalov Aleksandr Borisovich

Ushakov Nikolaj Mikhajlovich

Dates

2014-01-10Published

2012-05-11Filed