METHOD OF PRODUCING SILICATE GLASS WITH AMORPHOUS SILICON DIOXIDE-BASED REINFORCEMENT COATING Russian patent published in 2014 - IPC C03C17/30 

Abstract RU 2529071 C1

FIELD: chemistry.

SUBSTANCE: method includes synthesis of SiO2 sol, depositing SiO2 particles on silicate glass and heat treatment of the coated glass. An amorphous SiO2 based coating is applied by immersing silicate glass into SiO2 sol synthesised via hydrolysis of tetraethoxysilane using acetic acid (CH3COOH) as a synthesis reaction catalyst in a medium of ethyl alcohol (C2H5OH) in molar ratio of components tetraethoxysilane/H2O/C2H5OH/CH3COOH=0.05-0.25/0.95-2/2-16/0.05-0.25. The glass is drawn from the silicon dioxide sol at a controlled rate of 50 to 250 mm/min, followed by isothermal holding of the glass at a temperature of 500±10 to 600±10°C for 15±5 min.

EFFECT: method of producing glass with an amorphous silicon dioxide-based reinforcement coating.

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RU 2 529 071 C1

Authors

Es'Kin Stanislav Viktorovich

Zhimalov Alekandr Borisovich

Kosobudskij Igor' Donatovich

Ushakov Nikolaj Mikhajlovich

Dates

2014-09-27Published

2013-03-19Filed